Magnetic Resonance
Magnetic Resonance
MR
Articles | Volume 3, issue 2
Articles | Volume 3, issue 2
https://doi.org/10.5194/mr-3-183-2022
© Author(s) 2022. This work is distributed under
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/mr-3-183-2022
© Author(s) 2022. This work is distributed under
the Creative Commons Attribution 4.0 License.
Articles | Volume 3, issue 2
Research article
 | 
29 Sep 2022
Research article |  | 29 Sep 2022

Fine optimization of a dissolution dynamic nuclear polarization experimental setting for 13C NMR of metabolic samples

Arnab Dey, Benoît Charrier, Karine Lemaitre, Victor Ribay, Dmitry Eshchenko, Marc Schnell, Roberto Melzi, Quentin Stern, Samuel F. Cousin, James G. Kempf, Sami Jannin, Jean-Nicolas Dumez, and Patrick Giraudeau

Viewed

Total article views: 1,030 (including HTML, PDF, and XML)
HTML PDF XML Total BibTeX EndNote
751 258 21 1,030 13 8
  • HTML: 751
  • PDF: 258
  • XML: 21
  • Total: 1,030
  • BibTeX: 13
  • EndNote: 8
Views and downloads (calculated since 15 Jul 2022)
Cumulative views and downloads (calculated since 15 Jul 2022)

Viewed (geographical distribution)

Total article views: 1,030 (including HTML, PDF, and XML) Thereof 970 with geography defined and 60 with unknown origin.
Country # Views %
  • 1
1
 
 
 
 
Latest update: 28 May 2023
Download
Short summary
Nuclear magnetic resonance (NMR) is a great tool for analytical chemistry, but it is not the most sensitive one. This work aims to develop a sensitive and repeatable workflow for the analysis of complex samples by hyperpolarized 13C NMR. Through systematic and careful optimization of experimental parameters, we were able to achieve unprecedented sensitivity for the analysis of naturally abundant metabolite mixtures while maintaining the precision required for metabolomic studies.
Read more