Articles | Volume 1, issue 2
https://doi.org/10.5194/mr-1-155-2020
https://doi.org/10.5194/mr-1-155-2020
Research article
 | 
10 Jul 2020
Research article |  | 10 Jul 2020

Multiple solvent signal presaturation and decoupling artifact removal in 13C{1H} nuclear magnetic resonance

Marine Canton, Richard Roe, Stéphane Poigny, Jean-Hugues Renault, and Jean-Marc Nuzillard

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Status: closed
Status: closed
AC: Author comment | RC: Referee comment | SC: Short comment | EC: Editor comment
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Peer-review completion

AR: Author's response | RR: Referee report | ED: Editor decision
AR by Jean-Marc Nuzillard on behalf of the Authors (17 May 2020)  Manuscript 
ED: Publish as is (16 Jun 2020) by Marcel Utz
AR by Jean-Marc Nuzillard on behalf of the Authors (24 Jun 2020)
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Short summary
The cosmetic industry integrates in its products active ingredients of vegetal origin. For this purpose, plant extracts are prepared and their content must be characterized to check their conformity with safety regulations. Many plant extracts contain a high proportion of high-boiling-point solvents that may conflict with analytical protocols. Extract analysis by fractionation and subsequent 13C NMR analysis required a new solvent signal suppression technique to provide better analytical data.