Articles | Volume 1, issue 1
https://doi.org/10.5194/mr-1-97-2020
https://doi.org/10.5194/mr-1-97-2020
Research article
 | 
18 Jun 2020
Research article |  | 18 Jun 2020

Highly stable magic angle spinning spherical rotors

Thomas M. Osborn Popp, Alexander Däpp, Chukun Gao, Pin-Hui Chen, Lauren E. Price, Nicholas H. Alaniva, and Alexander B. Barnes

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Cited articles

Andrew, E. R.: Magic angle spinning, Int. Rev. Phys. Chem., 1, 195–224, https://doi.org/10.1080/01442358109353320, 1981. a, b
Andrew, E. R., Bradbury, A., and Eades, R. G.: Removal of dipolar broadening of nuclear magnetic resonance spectra of solids by specimen rotation, Nature, 183, 1802–1803, https://doi.org/10.1038/1831802a0, 1959. a
Bougault, C., Ayala, I., Vollmer, W., Simorre, J. P., and Schanda, P.: Studying intact bacterial peptidoglycan by proton-detected NMR spectroscopy at 100 kHz MAS frequency, J. Struct. Biol., 206, 66–72, https://doi.org/10.1016/j.jsb.2018.07.009, 2019. a
Bracewell, R. N. and Garriott, O. K.: Rotation of artificial Earth satellites, Nature, 182, 760–762, https://doi.org/10.1038/182760a0, 1958. a
Cegelski, L., Kim, S. J., Hing, A. W., Studelska, D. R., O'Connor, R. D., Mehta, A. K., and Schaefer, J.: Rotational-echo double resonance characterization of the effects of vancomycin on cell wall synthesis in Staphylococcus aureus, Biochemistry, 41, 13053–13058, https://doi.org/10.1021/bi0202326, 2002. a
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Short summary
We have recently demonstrated the capability to rapidly spin spherical rotors inclined precisely at the magic angle (54.74°) with respect to the external magnetic field used for nuclear magnetic resonance (NMR) experiments. We show that it is possible to spin a spherical rotor without using turbine grooves and that these rotors are extremely stable because of the inherent spherical-ring geometry. These results portend the facile implementation of spherical rotors for solid-state NMR experiments.