Articles | Volume 2, issue 1
https://doi.org/10.5194/mr-2-387-2021
https://doi.org/10.5194/mr-2-387-2021
Research article
 | 
04 Jun 2021
Research article |  | 04 Jun 2021

A novel sample handling system for dissolution dynamic nuclear polarization experiments

Thomas Kress, Kateryna Che, Ludovica M. Epasto, Fanny Kozak, Mattia Negroni, Gregory L. Olsen, Albina Selimovic, and Dennis Kurzbach

Viewed

Total article views: 2,248 (including HTML, PDF, and XML)
HTML PDF XML Total Supplement BibTeX EndNote
1,269 894 85 2,248 162 55 50
  • HTML: 1,269
  • PDF: 894
  • XML: 85
  • Total: 2,248
  • Supplement: 162
  • BibTeX: 55
  • EndNote: 50
Views and downloads (calculated since 02 Feb 2021)
Cumulative views and downloads (calculated since 02 Feb 2021)

Viewed (geographical distribution)

Total article views: 2,248 (including HTML, PDF, and XML) Thereof 2,048 with geography defined and 200 with unknown origin.
Country # Views %
  • 1
1
 
 
 
 

Cited

Latest update: 22 Jul 2024
Download
Short summary
We present a system for facilitated sample vitrification, melting, and transfer in dissolution dynamic nuclear polarization experiments. The system enables insertion of a sample through an airlock in combination with a dedicated dissolution system that is inserted through the same airlock shortly before the melting event. The cryostat can thus be operated continuously at low temperatures, and the melting process is rapid as no pressurization steps of the cryostat are necessary for dissolution.