Magnetic Resonance
Magnetic Resonance
MR
Articles | Volume 4, issue 2
Articles | Volume 4, issue 2
https://doi.org/10.5194/mr-4-199-2023
© Author(s) 2023. This work is distributed under
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/mr-4-199-2023
© Author(s) 2023. This work is distributed under
the Creative Commons Attribution 4.0 License.
Articles | Volume 4, issue 2
Research article
 | 
15 Aug 2023
Research article |  | 15 Aug 2023

Performance of the cross-polarization experiment in conditions of radiofrequency field inhomogeneity and slow to ultrafast magic angle spinning (MAS)

Andrej Šmelko, Jan Blahut, Bernd Reif, and Zdeněk Tošner

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Short summary
We present a tutorial on the cross-polarization experiment, which has been the main method of magnetization transfer in solid-state NMR for decades. We explain the principles of its volume-selective performance in the presence of magic angle spinning and radiofrequency field inhomogeneity and the decrease in efficiency with increasing sample rotation frequency.
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