Magnetic Resonance
Magnetic Resonance
MR
Articles | Volume 5, issue 1
Articles | Volume 5, issue 1
https://doi.org/10.5194/mr-5-1-2024
© Author(s) 2024. This work is distributed under
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/mr-5-1-2024
© Author(s) 2024. This work is distributed under
the Creative Commons Attribution 4.0 License.
Articles | Volume 5, issue 1
Research article
 | 
05 Jan 2024
Research article |  | 05 Jan 2024

Solid-state 13C-NMR spectroscopic determination of side-chain mobilities in zirconium-based metal–organic frameworks

Günter Hempel, Ricardo Kurz, Silvia Paasch, Kay Saalwächter, and Eike Brunner

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Short summary
Investigations of metal–organic frameworks are presented. This substance class is of interest for applications in gas storage (hydrogen, methane), separation, catalysis, and sensor technology. The properties of the material depend on the mobility of alkyl or alkyloxy side chains. We have determined that the side-chain methylene groups move highly anisotropically with a relatively short correlation time. Furthermore, we could improve the analysis procedure for the experiment used here.
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