Magnetic Resonance
Magnetic Resonance
MR
Articles | Volume 5, issue 2
Articles | Volume 5, issue 2
https://doi.org/10.5194/mr-5-121-2024
© Author(s) 2024. This work is distributed under
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/mr-5-121-2024
© Author(s) 2024. This work is distributed under
the Creative Commons Attribution 4.0 License.
Articles | Volume 5, issue 2
Research article
 | 
30 Aug 2024
Research article |  | 30 Aug 2024

1H-enhanced 103Rh NMR spectroscopy and relaxometry of 103Rh(acac)3 in solution

Harry Harbor-Collins, Mohamed Sabba, Markus Leutzsch, and Malcolm H. Levitt

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Short summary
The nuclear magnetic resonance (NMR) spectroscopy of the 103Rh nucleus is onerous owing to its dismal sensitivity. Here, we utilise modern techniques to boost the sensitivity and acquire valuable 103Rh NMR parameters for the Rh(acac)3 transition-metal complex. We acquire proton-enhanced 103Rh NMR spectra and successfully characterise the 103Rh spin relaxation. In doing so, we unveil the secrets of a complex that is of significant interest to the 103Rh NMR and wider chemical community alike.
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