Articles | Volume 5, issue 2
https://doi.org/10.5194/mr-5-153-2024
https://doi.org/10.5194/mr-5-153-2024
Research article
 | 
19 Nov 2024
Research article |  | 19 Nov 2024

Low-power WALTZ decoupling under magic-angle spinning NMR

Luzian Thomas and Matthias Ernst

Data sets

Low-Power WALTZ Decoupling under Magic-Angle Spinning Luzian Thomas and Matthias Ernst https://doi.org/10.3929/ethz-b-000697267

Model code and software

Low-Power WALTZ Decoupling under Magic-Angle Spinning Luzian Thomas and Matthias Ernst https://doi.org/10.3929/ethz-b-000697267

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Short summary
The paper investigates the suitability of an existing solution-state NMR spin decoupling sequence for use as a low-power solid-state NMR decoupling sequence under sample spinning. Complications arise from resonance conditions between the spin modulations by the pulse sequence and the sample rotation. We show that the timing of the pulse sequence is the most important criterion needed to achieve good decoupling. The paper gives recommendations for optimum parameters.