Bak, M. and Nielsen, N. C.: REPULSION, A Novel Approach to Efficient Powder Averaging in Solid-State NMR, J. Magn. Reson., 125, 132–139, https://doi.org/10.1006/jmre.1996.1087, 1997.
Barrie, P. J.: Distorted powder lineshapes in
27Al CP/MAS NMR
spectroscopy of solids, Chem. Phys. Lett., 208, 486–490,
https://doi.org/10.1016/0009-2614(93)87177-5, 1993.
Bayro, M. J., Huber, M., Ramachandran, R., Davenport, T. C., Meier, B. H.,
Ernst, M., and Griffin, R. G.: Dipolar truncation in magic-angle spinning
NMR recoupling experiments, J. Chem. Phys., 130, 114506, https://doi.org/10.1063/1.3089370, 2009.
Berruyer, P., Björgvinsdóttir, S., Bertarello, A., Stevanato, G.,
Rao, Y., Karthikeyan, G., Casano, G., Ouari, O., Lelli, M., Reiter, C.,
Engelke, F., and Emsley, L.: Dynamic Nuclear Polarization Enhancement of 200
at 21.15 T Enabled by 65 kHz Magic Angle Spinning, J. Phys. Chem. Lett., 11, 8386–8391,
https://doi.org/10.1021/acs.jpclett.0c02493, 2020.
Blanc, F., Sperrin, L., Jefferson, D. A., Pawsey, S., Rosay, M., and Grey,
C. P.: Dynamic Nuclear Polarization Enhanced Natural Abundance
17O
Spectroscopy, J. Am. Chem. Soc., 135, 2975–2978, https://doi.org/10.1021/ja4004377, 2013.
Brinkmann, A. and Edén, M.: Second order average Hamiltonian theory of symmetry-based pulse schemes in the nuclear magnetic resonance of rotating solids: Application to triple-quantum dipolar recoupling, J. Chem. Phys., 120, 11726–11745, https://doi.org/10.1063/1.1738102, 2004.
Brinkmann, A. and Kentgens, A. P. M.: Proton-Selective
17O-
1H
Distance Measurements in Fast Magic-Angle-Spinning Solid-State NMR
Spectroscopy for the Determination of Hydrogen Bond Lengths, J. Am. Chem. Soc., 128,
14758–14759, https://doi.org/10.1021/ja065415k, 2006a.
Brinkmann, A. and Kentgens, A. P. M.: Sensitivity Enhancement and Heteronuclear Distance Measurements in Biological
17O Solid-State NMR, J. Phys. Chem. B, 110, 16089–16101, https://doi.org/10.1021/jp062809p, 2006b.
Brinkmann, A. and Levitt, M. H.: Symmetry principles in the nuclear magnetic
resonance of spinning solids: Heteronuclear recoupling by generalized
Hartmann-Hahn sequences, J. Chem. Phys., 115, 357–384, https://doi.org/10.1063/1.1377031,
2001.
Brinkmann, A., Edén, M., and Levitt, M. H.: Synchronous helical pulse
sequences in magic-angle spinning nuclear magnetic resonance: double quantum
recoupling of multiple-spin systems, J. Chem. Phys.,112, 8539–8554,
https://doi.org/10.1063/1.481458, 2000.
Carravetta, M., Edén, M., Zhao, X., Brinkmann, A., and Levitt, M. H.:
Symmetry principles for the design of radiofrequency pulse sequences in the
nuclear magnetic resonance of rotating solids, Chem. Phys. Lett., 321, 205–215,
https://doi.org/10.1016/S0009-2614(00)00340-7, 2000.
Chen, J., Wu, X.-P., Hope, M. A., Qian, K., Halat, D. M., Liu, T., Li, Y.,
Shen, L., Ke, X., Wen, Y., Du, J.-H., Magusin, P. C. M. M., Paul, S., Ding,
W., Gong, X.-Q., Grey, C. P., and Peng, L.: Polar surface structure of oxide
nanocrystals revealed with solid-state NMR spectroscopy, Nat. Commun., 10, 1–10,
https://doi.org/10.1038/s41467-019-13424-7, 2019.
Ding, S. W. and Mcdowell, C. A.: Theoretical Calculations of the CPMAS
Spectral Lineshapes of Half-Integer Quadrupole Systems, J. Mag. Reson. A, 114, 80–87,
https://doi.org/10.1006/jmra.1995.1108, 1995.
Duong, N. T., Trébosc, J., Lafon, O., and Amoureux, J.-P.: Improved
sensitivity and quantification for
29Si NMR experiments on solids using
UDEFT (Uniform Driven Equilibrium Fourier Transform), Solid State Nucl. Magn. Reson., 100, 52–62,
https://doi.org/10.1016/j.ssnmr.2019.03.007, 2019.
Fernandez, C., Amoureux, J. P., Chezeau, J. M., Delmotte, L., and Kessler,
H.:
27Al MAS NMR characterization of AlPO
4-14 enhanced resolution
and information by MQMAS Dr. Hellmut G. Karge on the occasion of his 65th
birthday, Microporous Mater., 6, 331–340, https://doi.org/10.1016/0927-6513(96)00040-5, 1996.
Freeman, R., Kempsell, S. P., and Levitt, M. H.: Radiofrequency pulse
sequences which compensate their own imperfections, J. Magn. Reson., 38, 453–479,
https://doi.org/10.1016/0022-2364(80)90327-3, 1980.
Gansmüller, A., Simorre, J.-P., and Hediger, S.: Windowed R-PDLF
recoupling: A flexible and reliable tool to characterize molecular dynamics,
J. Magn. Reson., 234, 154–164, https://doi.org/10.1016/j.jmr.2013.06.017, 2013.
Garwood, M. and DelaBarre, L.: The Return of the Frequency Sweep: Designing
Adiabatic Pulses for Contemporary NMR, J. Magn. Reson., 153, 155–177,
https://doi.org/10.1006/jmre.2001.2340, 2001.
Giovine, R., Trébosc, J., Pourpoint, F., Lafon, O., and Amoureux, J.-P.:
Magnetization transfer from protons to quadrupolar nuclei in solid-state NMR
using PRESTO or dipolar-mediate
d refocused INEPT methods, J. Magn. Reson., 299, 109–123,
https://doi.org/10.1016/j.jmr.2018.12.016, 2019.
Gómez, J. S., Rankin, A. G. M., Trébosc, J., Pourpoint, F., Tsutsumi, Y., Nagashima, H., and Lafon, O.: Improved NMR transfer of magnetization from protons to half-integer spin quadrupolar nuclei at moderate and high MAS frequencies, Zenodo [data set], https://doi.org/10.5281/zenodo.4896852, 2021.
Harris, R. K. and Nesbitt, G. J.: Cross polarization for quadrupolar
nuclei – Proton to sodium-23, J. Magn. Reson., 78, 245–256,
https://doi.org/10.1016/0022-2364(88)90268-5, 1988.
Hayashi, S. and Hayamizu, K.: Line shapes in CP/MAS NMR spectra of
half-integer quadrupolar nuclei, Chem. Phys. Lett., 203, 319–324,
https://doi.org/10.1016/0009-2614(93)85575-9, 1993.
Hope, M. A., Halat, D. M., Magusin, P. C. M. M., Paul, S., Peng, L., and
Grey, C. P.: Surface-selective direct
17O DNP NMR of CeO
2
nanoparticles, Chem. Commun., 53, 2142–2145, https://doi.org/10.1039/C6CC10145C, 2017.
Hu, B., Delevoye, L., Lafon, O., Trébosc, J., and Amoureux, J. P.:
Double-quantum NMR spectroscopy of 31P species submitted to very large CSAs,
J. Magn. Reson., 200, 178–88, https://doi.org/10.1016/j.jmr.2009.06.020, 2009.
Hwang, S.-J., Chen, C.-Y., and Zones, S. I.: Boron Sites in Borosilicate
Zeolites at Various Stages of Hydration Studied by Solid State NMR
Spectroscopy, J. Phys. Chem. B, 108, 18535–18546, https://doi.org/10.1021/jp0476904, 2004.
Kervern, G., Pintacuda, G., and Emsley, L.: Fast adiabatic pulses for solid-state NMR of paramagnetic systems, Chem. Phys. Lett., 435, 157–162, https://doi.org/10.1016/j.cplett.2006.12.056, 2007.
Lee, D., Duong, N. T., Lafon, O., and De Paëpe, G.: Primostrato Solid-State NMR Enhanced by Dynamic Nuclear Polarization: Pentacoordinated Al
3+ Ions Are Only Located at the Surface of Hydrated
γ-Alumina, J. Phys. Chem. C, 118, 25065–25076, https://doi.org/10.1021/jp508009x, 2014.
Lee, D., Leroy, C., Crevant, C., Bonhomme-Coury, L., Babonneau, F.,
Laurencin, D., Bonhomme, C., and Paëpe, G. D.: Interfacial Ca
2+
environments in nanocrystalline apatites revealed by dynamic nuclear
polarization enhanced
43Ca NMR spectroscopy, Nat. Commun., 8, 14104,
https://doi.org/10.1038/ncomms14104, 2017.
Levitt, M. H.: Symmetry-based pulse sequences in magic-angle spinning
solid-state NMR, in: Encyclopedia of Nuclear Magnetic Resonance. Volume 9,
Advances in NMR, edited by: Grant, D. M. and Harris, R. K., Wiley, Chichester, UK, 165–196,
2002.
Levitt, M. H. and Freeman, R.: NMR population inversion using a composite pulse, J. Magn. Reson., 33, 473–476, https://doi.org/10.1016/0022-2364(79)90265-8, 1979.
Li, W., Wang, Q., Xu, J., Aussenac, F., Qi, G., Zhao, X., Gao, P., Wang, C.,
and Deng, F.: Probing the surface of
γ-Al
2O
3 by oxygen-17
dynamic nuclear polarization enhanced solid-state NMR spectroscopy, Phys. Chem. Chem. Phys., 20,
17218–17225, https://doi.org/10.1039/C8CP03132K, 2018.
Liang, L., Hou, G., and Bao, X.: Measurement of proton chemical shift
anisotropy in solid-state NMR spectroscopy, Solid State Nucl. Magn. Reson., 93, 16–28,
https://doi.org/10.1016/j.ssnmr.2018.04.002, 2018.
Lu, X., Lafon, O., Trébosc, J., Tricot, G., Delevoye, L., Méar, F.,
Montagne, L., and Amoureux, J. P.: Observation of proximities between
spin-
and quadrupolar nuclei: which heteronuclear dipolar recoupling
method is preferable?, J. Chem. Phys.,137, 144201, https://doi.org/10.1063/1.4753987,
2012.
Madhu, P. K., Zhao, X., and Levitt, M. H.: High-resolution
1H NMR in
the solid state using symmetry-based pulse sequences, Chem. Phys. Lett., 346, 142–148,
https://doi.org/10.1016/S0009-2614(01)00876-4, 2001.
Mao, K., Wiench, J. W., Lin, V. S.-Y., and Pruski, M.: Indirectly detected
through-bond chemical shift correlation NMR spectroscopy in solids under
fast MAS: Studies of organic–inorganic hybrid materials, J.
Magn. Reson., 196, 92–95, https://doi.org/10.1016/j.jmr.2008.10.010,
2009.
Martineau, C., Bouchevreau, B., Taulelle, F., Trébosc, J., Lafon, O.,
and Amoureux, J. P.: High-resolution through-space correlations between
spin-
and half-integer quadrupolar nuclei using the MQ-D-R-INEPT NMR
experiment, Phys. Chem. Chem. Phys., 14, 7112–7119, https://doi.org/10.1039/C2CP40344G, 2012.
Morris, H. D. and Ellis, P. D.: Aluminum-27 cross polarization of aluminas.
The NMR spectroscopy of surface aluminum atoms, J. Am. Chem. Soc., 111, 6045–6049,
https://doi.org/10.1021/ja00198a012, 1989.
Nagashima, H., Lilly Thankamony, A. S., Trébosc, J., Montagne, L.,
Kerven, G., Amoureux, J.-P., and Lafon, O.: Observation of proximities
between spin-
and quadrupolar nuclei in solids: Improved robustness to
chemical shielding using adiabatic symmetry-based recoupling, Solid State Nucl. Magn. Reson., 94, 7–19,
https://doi.org/10.1016/j.ssnmr.2018.07.001, 2018.
Nagashima, H., Trébosc, J., Kon, Y., Sato, K., Lafon, O., and Amoureux,
J.-P.: Observation of Low-
γ Quadrupolar Nuclei by Surface-Enhanced
NMR Spectroscopy, J. Am. Chem. Soc., 142, 10659–10672,
https://doi.org/10.1021/jacs.9b13838, 2020.
Nagashima, H., Trébosc, J., Kon, Y., Lafon, O., and Amoureux, J.-P.: Efficient transfer of DNP-enhanced
1H magnetization to half-integer quadrupolar nuclei in solids at moderate spinning rate, Magn. Reson. Chem., https://doi.org/10.1002/mrc.5121, online first, 2021.
Pandey, M. K., Malon, M., Ramamoorthy, A., and Nishiyama, Y.:
Composite-180
∘ pulse-based symmetry sequences to recouple proton
chemical shift anisotropy tensors under ultrafast MAS solid-state NMR
spectroscopy, J. Magn. Reson., 250, 45–54, https://doi.org/10.1016/j.jmr.2014.11.002,
2015.
Peng, L., Huo, H., Liu, Y., and Grey, C. P.:
17O Magic Angle Spinning
NMR Studies of Brønsted Acid Sites in Zeolites HY and HZSM-5, J. Am. Chem. Soc., 129,
335–346, https://doi.org/10.1021/ja064922z, 2007.
Perras, F. A., Kobayashi, T., and Pruski, M.: Natural Abundance
17O DNP
Two-Dimensional and Surface-Enhanced NMR Spectroscopy, J. Am. Chem. Soc., 137, 8336–8339,
https://doi.org/10.1021/jacs.5b03905, 2015a.
Perras, F. A., Kobayashi, T., and Pruski, M.: PRESTO polarization transfer
to quadrupolar nuclei: implications for dynamic nuclear polarization, Phys. Chem. Chem. Phys., 17,
22616–22622, https://doi.org/10.1039/C5CP04145G, 2015b.
Perras, F. A., Chaudhary, U., Slowing, I. I., and Pruski, M.: Probing
Surface Hydrogen Bonding and Dynamics by Natural Abundance,
Multidimensional,
17O DNP-NMR Spectroscopy, J. Phys. Chem. C, 120, 11535–11544,
https://doi.org/10.1021/acs.jpcc.6b02579, 2016.
Perras, F. A., Wang, Z., Naik, P., Slowing, I. I., and Pruski, M.: Natural
Abundance
17O DNP NMR Provides Precise O-H Distances and Insights into
the Brønsted Acidity of Heterogeneous Catalysts, Angew. Chem. Int. Ed., 56, 9165–9169,
https://doi.org/10.1002/anie.201704032, 2017.
Perras, F. A., Goh, T. W., Wang, L.-L., Huang, W., and Pruski, M.: Enhanced
1H-X D-HMQC performance through improved 1H homonuclear decoupling, Solid State Nucl. Magn. Reson., 98,
12–18, https://doi.org/10.1016/j.ssnmr.2019.01.001, 2019.
Pileio, G., Concistrè, M., McLean, N., Gansmüller, A., Brown, R. C.
D., and Levitt, M. H.: Analytical theory of
γ-encoded double-quantum
recoupling sequences in solid-state nuclear magnetic resonance, J. Magn. Reson., 186,
65–74, https://doi.org/10.1016/j.jmr.2007.01.009, 2007.
Rankin, A. G. M., Trébosc, J., Pourpoint, F., Amoureux, J.-P., and
Lafon, O.: Recent developments in MAS DNP-NMR of materials, Solid State Nucl. Magn. Reson., 101, 116–143,
https://doi.org/10.1016/j.ssnmr.2019.05.009, 2019.
Rocha, J., Carr, S. W., and Klinowski, J.:
27Al quadrupole nutation and
1H-
27Al cross-polarization solid-state NMR studies of ultrastable
zeolite Y with fast magic-angle spinning, Chem. Phys. Lett., 187, 401–408,
https://doi.org/10.1016/0009-2614(91)80272-Y, 1991.
Tricot, G., Lafon, O., Trébosc, J., Delevoye, L., Méar, F.,
Montagne, L., and Amoureux, J.-P.: Structural characterisation of phosphate
materials: new insights into the spatial proximities between phosphorus and
quadrupolar nuclei using the D-HMQC MAS NMR technique, Phys. Chem. Chem. Phys., 13, 16786–16794,
https://doi.org/10.1039/C1CP20993K, 2011.
Vega, A. J.: CPMAS of quadrupolar
S = nuclei, Solid State Nucl. Magn. Reson., 1, 17–32,
https://doi.org/10.1016/0926-2040(92)90006-U, 1992.
Vitzthum, V., Mieville, P., Carnevale, D., Caporini, M. A., Gajan, D.,
Copéret, C., Lelli, M., Zagdoun, A., Rossini, A. J., Lesage, A., Emsley,
L., and Bodenhausen, G.: Dynamic nuclear polarization of quadrupolar nuclei
using cross polarization from protons: surface-enhanced aluminium-27 NMR,
Chem. Commun., 48, 1988–1990, https://doi.org/10.1039/c2cc15905h, 2012.
Vogt, F. G., Yin, H., Forcino, R. G., and Wu, L.:
17O Solid-State NMR
as a Sensitive Probe of Hydrogen Bonding in Crystalline and Amorphous Solid
Forms of Diflunisal, Mol. Pharmaceutics, 10, 3433–3446, https://doi.org/10.1021/mp400275w,
2013.
Wittmann, J. J., Mertens, V., Takeda, K., Meier, B. H., and Ernst, M.:
Quantification and compensation of the influence of pulse transients on
symmetry-based recoupling sequences, J. Magn. Reson., 263,
7–18, https://doi.org/10.1016/j.jmr.2015.12.011, 2016.
Zhao, X., Edén, M., and Levitt, M. H.: Recoupling of heteronuclear dipolar interactions in solid-state NMR using symmetry-based pulse sequences, Chem. Phys. Lett., 342, 353–361, https://doi.org/10.1016/S0009-2614(01)00593-0, 2001.
Zhao, X., Hoffbauer, W., Schmedt auf der Günne, J., and Levitt, M. H.:
Heteronuclear polarization transfer by symmetry-based recoupling sequences
in solid-state NMR, Solid State Nucl. Magn. Res., 26, 57–64,
https://doi.org/10.1016/j.ssnmr.2003.11.001, 2004.