Articles | Volume 2, issue 2
https://doi.org/10.5194/mr-2-589-2021
https://doi.org/10.5194/mr-2-589-2021
Research article
 | 
04 Aug 2021
Research article |  | 04 Aug 2021

Efficient polynomial analysis of magic-angle spinning sidebands and application to order parameter determination in anisotropic samples

Günter Hempel, Paul Sotta, Didier R. Long, and Kay Saalwächter

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Interactive discussion

Status: closed

Comment types: AC – author | RC – referee | CC – community | EC – editor | CEC – chief editor | : Report abuse
  • CC1: 'Comment on mr-2021-39 from the NMR Dept., Institute of Macromolecular Chemistry, Prague', Jiří Czernek, 09 Apr 2021
    • AC1: 'Reply on CC1', Günter Hempel, 24 Jun 2021
  • RC1: 'Comment on mr-2021-39', Anonymous Referee #1, 19 May 2021
    • AC2: 'Reply on RC1', Günter Hempel, 28 Jun 2021
      • AC4: 'Reply on AC2', Günter Hempel, 29 Jun 2021
  • RC2: 'Comment on mr-2021-39', Anonymous Referee #2, 15 Jun 2021
    • AC3: 'Reply on RC2', Günter Hempel, 28 Jun 2021

Peer review completion

AR: Author's response | RR: Referee report | ED: Editor decision
AR by Günter Hempel on behalf of the Authors (13 Jul 2021)  Author's response    Author's tracked changes    Manuscript
ED: Publish as is (15 Jul 2021) by Perunthiruthy Madhu
AR by Günter Hempel on behalf of the Authors (16 Jul 2021)  Author's response    Manuscript
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Short summary
We develop an exact analytical description of spinning sideband intensities in magic-angle spinning NMR, e.g., for 13C CSA. This can be used in spectral fitting to obtain tensor parameters and plays out its advantage in the analysis of orientation effects in non-isotropic samples. We present an improved approach to process data obtained with the simple syncMAS experiment, which is powerful but not very popular due to the as yet not very transparent and difficult data analysis.