Articles | Volume 5, issue 2
https://doi.org/10.5194/mr-5-167-2024
https://doi.org/10.5194/mr-5-167-2024
Research article
 | 
20 Nov 2024
Research article |  | 20 Nov 2024

Workflow for systematic design of electrochemical in operando NMR cells by matching B0 and B1 field simulations with experiments

Michael Schatz, Matthias Streun, Sven Jovanovic, Rüdiger-A. Eichel, and Josef Granwehr

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Interactive discussion

Status: closed

Comment types: AC – author | RC – referee | CC – community | EC – editor | CEC – chief editor | : Report abuse
  • RC1: 'Comment on mr-2024-12', Anonymous Referee #1, 17 Aug 2024
    • AC1: 'Reply on RC1', Michael Schatz, 30 Aug 2024
  • RC2: 'Comment on mr-2024-12', Anonymous Referee #2, 18 Aug 2024
    • AC2: 'Reply on RC2', Michael Schatz, 30 Aug 2024
  • RC3: 'Comment on mr-2024-12', Bruce Balcom, 05 Sep 2024
    • AC3: 'Reply on RC3', Michael Schatz, 02 Oct 2024

Peer review completion

AR: Author's response | RR: Referee report | ED: Editor decision | EF: Editorial file upload
AR by Josef Granwehr on behalf of the Authors (05 Sep 2024)  Author's response   Author's tracked changes   Manuscript 
ED: Publish as is (06 Sep 2024) by Jan Gerrit Korvink
AR by Michael Schatz on behalf of the Authors (02 Oct 2024)  Author's response   Manuscript 
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Short summary
We developed a workflow using finite element methods to optimise electrochemical cell designs for in operando nuclear magnetic resonance by accurately matching magnetic field and radio frequency field simulations with experimental data. Guidelines for enhanced sensitivity and field homogeneity are given. A radio frequency amplification effect in coin cells is described by empirical formulae, which have the potential to improve spatial selectivity in future in operando applications.