Magnetic Resonance
Magnetic Resonance
MR
Articles | Volume 2, issue 2
Articles | Volume 2, issue 2
https://doi.org/10.5194/mr-2-571-2021
© Author(s) 2021. This work is distributed under
the Creative Commons Attribution 4.0 License.
Special issue:
https://doi.org/10.5194/mr-2-571-2021
© Author(s) 2021. This work is distributed under
the Creative Commons Attribution 4.0 License.
Articles | Volume 2, issue 2
Research article
 | 
12 Jul 2021
Research article |  | 12 Jul 2021

Rapid measurement of heteronuclear transverse relaxation rates using non-uniformly sampled R1ρ accordion experiments

Sven Wernersson, Göran Carlström, Andreas Jakobsson, and Mikael Akke

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Latest update: 19 Apr 2024
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Short summary
Multidimensional NMR relaxation experiments provide a powerful means of studying protein dynamics but typically require long acquisition times. Here, we combine two approaches that individually shorten the length of the experiment: accordion spectroscopy and non-uniform sampling (NUS). We extract relaxation rate constants by applying maximum likelihood estimation of sparse exponential modes modeled on the accordion–NUS interferograms, resulting in time savings by a factor of roughly 10.
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