Centre de Résonance Magnétique Nucléaire à Très
Hauts Champs – FRE 2034 Université de Lyon/CNRS/Université
Claude Bernard Lyon 1/ENS de Lyon, 5 Rue de la Doua, 69100 Villeurbanne,
France
current address: Department of Chemistry, University of Liverpool, Liverpool L69 7ZD, United Kingdom
Quentin Stern
Centre de Résonance Magnétique Nucléaire à Très
Hauts Champs – FRE 2034 Université de Lyon/CNRS/Université
Claude Bernard Lyon 1/ENS de Lyon, 5 Rue de la Doua, 69100 Villeurbanne,
France
Sami Jannin
Centre de Résonance Magnétique Nucléaire à Très
Hauts Champs – FRE 2034 Université de Lyon/CNRS/Université
Claude Bernard Lyon 1/ENS de Lyon, 5 Rue de la Doua, 69100 Villeurbanne,
France
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A straightforward line shape analysis of the 13C NMR spectra of [2-13C]sodium acetate can be used to indirectly evaluate the 13H polarization of the CH3 group and likely entire samples in the case of rapid and homogeneous 13H–1H spin diffusion. The results are potentially advantageous for polarizers that lack 1H radiofrequency hardware, measurements that are influenced by radiation damping or large background signals, or where acquisition of thermal equilibrium spectra is not feasible.
A straightforward line shape analysis of the 13C NMR spectra of [2-13C]sodium acetate can be...
