Magnetic Resonance
Magnetic Resonance
MR
Articles | Volume 4, issue 1
Articles | Volume 4, issue 1
https://doi.org/10.5194/mr-4-153-2023
© Author(s) 2023. This work is distributed under
the Creative Commons Attribution 4.0 License.
https://doi.org/10.5194/mr-4-153-2023
© Author(s) 2023. This work is distributed under
the Creative Commons Attribution 4.0 License.
Articles | Volume 4, issue 1
Research article
 | 
05 Jun 2023
Research article |  | 05 Jun 2023

The solid effect of dynamic nuclear polarization in liquids

Deniz Sezer

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Cited articles

Abragam, A.: The Principles of Nuclear Magnetism, Oxford University Press, New York, ISBN 978 0 19 852014 6, 1961. a, b, c
Abragam, A. and Proctor, W. G.: Une nouvelle méthode de polarisation dynamique des noyaux atomiques dans les solides, Compt. rend., 246, 2253–2256, 1958. a
Anderson, P. W.: A Mathematical Model for the Narrowing of Spectral Lines by Exchange or Motion, J. Phys. Soc. Jpn., 9, 316–339, https://doi.org/10.1143/JPSJ.9.316, 1954. a
Ayant, Y., Belorizky, E., Alizon, J., and Gallice, J.: Calcul des densit'es spectrales r'esultant d'un mouvement al'eatoire de translation en relaxation par interaction dipolaire magn'etique dans les liquides, J. Phys., 36, 991–1004, 1975. a, b, c, d, e
Delage-Laurin, L., Palani, R. S., Golota, N., Mardini, M., Ouyang, Y., Tan, K. O., Swager, T. M., and Griffin, R. G.: Overhauser Dynamic Nuclear Polarization with Selectively Deuterated BDPA Radicals, J. Am. Chem. Soc., 143, 20281–20290, https://doi.org/10.1021/jacs.1c09406, 2021. a
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We show that the field profile of the solid effect in liquids is rich in dynamical information, including about timescales of molecular diffusion. We develop a general theoretical framework for extracting this information through quantitative fits to the experimental data. Unusual peaks in the enhancement field profile, which resemble thermal mixing but are not related to it, are demonstrated to arise in liquids under some conditions. These additionally restrict the dynamical parameters.
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